Gram-Scale High-Throughput Organic Synthesis Workstation
Gram-Scale High-Throughput Organic Synthesis Workstation
Gram-Scale High-Throughput Organic Synthesis Workstation
This intelligent experimental platform is designed for gram-scale, high-throughput organic synthesis. It enables precise dosing of organic reagents, inorganic acids, and bases, followed by temperature-controlled stirring reactions. Integrated purification workflows, including quenching, extraction, filtration, column chromatography, recrystallization, and concentration, are available for gram-scale organic material preparation. The system supports process optimization, synthetic route screening, and batch preparation. With a high degree of automation, it balances experimental throughput and data accuracy, making it suitable for small-molecule synthesis in the pharmaceutical, fine chemical, and organic optoelectronic fields.
Features
- Wide Applicability and Flexibility
Full-process coverage for both solid and liquid reagents. Compatible with high/low temperature and anhydrous/oxygen-free conditions; scalable batch size and adjustable parameters.
- Stable Automatic Operation
Minimized manual intervention reduces operational errors and improves repeatability and batch-to-batch consistency for high-throughput R&D.
- Safe and Robust
An enclosed, programmable workflow isolates hazardous atmospheres and reagents, ensuring operator protection and stable experimental output.
Specifications
|
Module |
Item |
Parameters |
Module |
|
Dosing Unit |
Reaction Vessels |
Pear Shaped Flasks |
25,100,250 mL (general used);500 mL |
|
Test Tubes |
20 mL |
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Solid Collection Vials |
5 mL(φ22×50 mm), 25g(φ50×84 mm) |
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Pre NMR Vials |
4 mL |
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|
Solid Dosing |
Raw Material Stations |
3 stations, 96 vessels per station (standard pipette tip rack) |
|
|
Negative Pressure Dosing |
Tens of milligrams to several grams |
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|
Scale |
6 positions, compatible with 20 mL reagent bottle caps |
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Liquid Dosing |
Syringe Pump |
2 positions, 1 μL precision |
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|
Pipette |
1000 μL |
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Capping & decapping Module |
Magnetic Capping Jaw |
Compatible vessels: 250 mL / 125 mL / 30 mL / 5 mL reagent bottles; 100 g / 25 g solid stock vials; 4 mL pre NMR vials |
|
|
Reaction Module |
Stirring Module |
Magnetic Stirring & Heating |
Speed ＞1200 rpm, temperature range ambient to 200 ℃, six positions with independent temperature control |
|
Magnetic Stirring with Cooling |
Speed ＞1200 rpm, cooling circulation temperature 10–30 ℃ |
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Standalone Magnetic Stirring: |
Speed ＞1200 rpm, automatic stir bar loading and retrieval supported |
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|
Processing Module |
Separation Module |
Separatory Funnels |
125,250,500 mL |
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Filter Funnels |
12,40,120 g |
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Flash Chromatography System |
Silica columns 12 g / 40 g / 120 g, automatic solid loading |
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Fraction Collector |
3 tray positions, compatible with 20 mL test tubes |
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Concentration Module |
Rotary Evaporator |
Ambient to 100 ℃; condenser temperature −20 ℃ to ambient; controllable vacuum |
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Vacuum Drying Oven |
Ambient to 150 ℃, automatic door opening and closing |
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Drying Module |
Vacuum Oil Pump |
Equipped with oil water separator |
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Weighing Balance |
Readability 1 mg |
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Cleaning & Post Treatment |
Ultrasonic Cleaning |
Ultrasonic Cleaning |
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Scraping & Grinding Module |
Feature |
Independent automatic scraping module |
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Overall System Specifications |
Configuration |
Glove box + functional pretreatment platform + central six axis robotic arm |
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Overall Dimension |
5m×8m |
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